Volume 30, Issue 1 (Jun 2011)                   jame 2011, 30(1): 1-11 | Back to browse issues page


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J. Jaafaripour Maybody, E. Salahi, A. Nemati, M.H. Amin. In-situ Preparation of Hydroxyapatite-Carbon Nanotubes Nanocomposite and Investigation of its Microstructure and Morphology. jame. 2011; 30 (1) :1-11
URL: http://jame.iut.ac.ir/article-1-517-en.html

Department of Materials Engineering, Science and Research Branch Islamic Azad University, Tehran, Iran
Abstract:   (3361 Views)
In the present study, in-situ synthesis of carbon nanotube/hydroxyapatite nano composite powder with stable homogeneous dispersions of carbon nanotubes (CNTs) was carried out using surfactant as dispersing agent. By applying sol-gel method, dispersion in the hydroxyapatite matrix and its effects on the microstructure were investigated. The chemical and phase composition, structure and morphological and size analyses were performed using XRD, FT-IR, SEM, TEM/SAED/EDX, Raman, UV-Vis spectroscopy and differential scanning calorimetry (DSC). The influences of different dispersing agents (sodium dodecyl sulfate, SDS) as a benchmark for future dispersion experiments) and excitation wavelength are discussed and the results are compared to the commonly used UV-Visible spectroscopic analysis. The results indicated that synthesis of hydroxyapatite particles in the presence of the carbon nanotubes had the best homogenization of the carbon nanotube dispersion and faster crystallization of hydroxyapatite, and the use of SDS for dispersion carbon nanotubes at hydroxyapatite matrix rendered formation of hydroxyapatite coating on CNTs surface. The average crystallite size of heat-treated (at 600°C) samples, estimated by Scherrer,s equation, was found to be ~50-60 nm that was confirmed by TEM.
Full-Text [PDF 1764 kb]   (1585 Downloads)    
Type of Study: Research | Subject: General
Received: 2015/02/9 | Accepted: 2015/05/5 | Published: 2015/05/5

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