Evaluating the Effect of Ta/W Ratio on Microstructure and Stress Rupture Properties of Ni-Based Single Crystal Superalloy PWA1483

Authors

1 1- Materials Engineering Group, Pardis College, Isfahan University of Technology, Isfahan 84156-83111, Iran. 2- Department of Materials Engineering, Isfahan University of Technology, Isfahan 84156-83111, Iran.

2 Department of Materials Engineering, Isfahan University of Technology, Isfahan 84156-83111, Iran.

Abstract

In this study, the effect of Ta/W ratio on the microstructure and stress rupture properties of Ni-based single crystal (SX) superalloy PWA1483 was investigated. For this purpose, single crystal (SX) superalloys with different Ta/W ratios (0.75, 1.0, 1.32 and 1.5 in wt.%) were fabricated. The alloys were directionally solidified by Bridgman method under the same solidification condition at withdrawal velocity of 3 mm/min and thermal gradient of about 7 K/mm followed by standard age hardening heat treatment. Microstructural characterization was performed using optical microscopy (OM) and scanning electron microscopy (SEM). The stress rupture properties were investigated at 982 °C and 248 MPa. The results showed that increasing the Ta/W ratio decreases the size and volume fraction of micro-pores together with the size of γ' precipitates. Hence, the stress rupture life increased. The superalloy with Ta/W ratio of 1.5 showed the minimum size of micro-porosity (18.2 μm) and the maximum stress rupture life (~34 h). The superalloy with Ta/W ratio of 1 showed the most uniform microstructure and creep behavior. It seems that the presence of topologically closed packed (TCP) η-phases is the main reason for stress rupture life decrease in SX superalloy as micro-pores initiated from TCP phases or the TCP/matrix interfaces.
 
 

Keywords


1. Zhang, S., and Zhao, D., Aeraospace Materials Handbook, Advancces in Materials and Engineering, CRC Press, 2012.
2. Pollock, T. M., and Tin, S., “Nickel-Based Superalloys for Advanced Turbine Engines: Chemistry, Microstructure and Properties”, J. Propuls. Power, Vol. 22, pp. 361-374, 2006.
3. Ruttert, B., Meid, C., Lopez-Galilea, L. M. I., Bartsch, M., and Theisen, W., “Effect of Porosity and Eutectics on the High-Temperature Low-Cycle Fatigue Performance of a Nickel-Based Single Crystal Superalloys”, Scripta Materials, Vol. 140, pp. 139-143, 2018.
4. Zhang, Y. B., Liu, L., Huang, T. W., Li, Y. F., Jie, Z. Q., Zhang, J., Yang, W. C., and Fu, H. Z., “Investigation on Remelting Solution Heat Treatment for Nickel-Based Single Crystal Superalloys”, Scripta Materials, No. 136, pp. 74-77, 2017.
5. Li, X. W., Wang, L., Dong, J. S., Lou, L., and Zhang, H. J., “Evolution of Micro-Pores in a Single Crystal Nickel-Based Superalloy During Solution Heat Treatment”, Metals and Materials Transactions, A, No. 48, pp. 2682-2685, 2017.
6. Xuan, W., Du, L., Han, Y., Shao, W., Zhang, H., Wang, J., Ren, Z., and Zhong, Y., “Investigation on Microstructure and Creep Properties of Nickel- Based Single Crystal Superalloys PWA1483 During Heat Treatment under an Alternating Magnetic Field”, Materials Science and Engineering A, No. 762, Article. 138087, 2019.
7. Wasson, A. J., “The Impact of Carbon on Single Crystal Nickel Based Superalloys: Carbide Behavior and Alloy Performance”, Ph.D. Thesis, University of Florida, 2010.
8. Matuszewski, K., Precipitation of Topologically Close Packed Phases in Ni-Base Superalloys -the Effect of Re and Ru, Erlangen FAU University Press, 2016.
9. Zhang, Y., and Li, J., “Characterization of the Microstructure Evolution and Microsegregation in a Ni-Based Superalloy under Super-High Thermal Gradient Directional Solidification”, Materials Transactions, Vol. 53, No. 11, pp. 1910-1914, 2012.
10. Yamagata, T., Harada, H., Nakazawa, S., and Yamazaki, M., “Effect of Ta/W Ratio in Gama Prime Phase on Creep Strength of Nickel-Base Single Crystal Superalloys”, Transactions, The Iron and Steel Institute of Japan (ISIJ), Vol. 26, pp. 638-641, 1986.
11. Sugui, T., Minggang, W., Xingfu, Y., Xudong, L., and Benjiang, Q., “Directional Diffusion and Effect Factors of the Elements During Creep of Nickel-Based Single Crystal Superalloys”, Materials Science Forum, Vols. 638-642, pp. 2339-2344, 2010.
12. Lamm, M., and Singer, R. F., “The Effect of Casting Conditions on the High-Cycle Fatigue Properties of the Single-Crystal Ni-Base Superalloy PWA 1483”, Metallurgical and Materials Transaction A, Vol. 38A, pp. 1177-1183, 2007.
13. Gancarczyk, K., Albrecht, R., Berger, H., Szeliga, D., Gradzik, A., and Sieniawski, J., “Determination of Crystal Orientation by X-Scan Method in Nickel-Based Single-Crystal Turbine Blades”, Metallurgical and Materials Transaction A, Vol. 48, pp. 5200-5205, 2017.
14. Goti, R., Viguier, B., and Crabos, F., “Effect of Thermal Cycling on High Temperature Creep of Coated CMSX-4”, Superalloys, 2012: 12th International Symposium on Superalloys, TMS (The Minerals, Metals & Materials Society), pp. 411-419, 2012.
15. Wahl, J. B., and Harris, K., “CMSX-4 Plus Single Crystal Alloy Development: Characterization and Application Development”, Superalloys, 2016: Proceedings of the 13th International Symposium on Superalloys, TMS (The Minerals, Metals & Materials Society), pp. 25-33, 2016.
16. Ma, D., Wang, F., Wu, Q., Bogner, S., and Polaczek, A. B., “Innovations in Casting Techniques for Single Crystal Turbine Blades of Superalloys”, Superalloys, 2016: Proceedings of the 13th International Symposium on Superalloys, TMS (The Minerals, Metals & Materials Society), pp. 237-246, 2016.
17. Sadeghi, F., Kermanpur, A., Sarami, N., and Riazi, H., “Investigation the Effect of Crystal Orientation of a Single Crystal Superalloy on High Temperature Mechanical Properties”, 5th International Conference on Materials Engineering and Metallurgy, Shiraz University, 2016.
18. Standard Test Method for Determining Volume Fraction by Systematic Manual Point Count, ASTM Standards 2008, West Conshohoken, PA : ASTM International, 2008.
19. AMS 2315 D Standard, Standard Test Method for Determination of Delta Ferrite Content, American National Standard, 1995.
20. ASTM E 139-00 Standard, Standard Test Methods for Conducting Creep, Creep-Rupture, and Stress-Rupture Tests of Metallic Materials, ASTM International, United States, 2000.
21. Erickson, G. L., Kubiak, K., and Sieniawski, J., “The Development and Application of CMSX-10”, The Minerals, Metals and Materials Society, pp. 35-44, 1996.
22. Shah, D. M., Cetel, A., and Hartford, E., “Evaluation of PWA1483 for Large Single Crystal IGT Blade Applications”, The Minerals, Metals and Materials Society ( TMS), pp. 295-304, 2000.
23. Vacchieri, E., and Costa, A., “Comparison of the Mechanical Behavior and Evaluation of Different Damage Mechanisms in an Equiaxed and a Single Crystal Superalloys Subjected to Creep, LCF and TMF”, 12th International Symposium on Superalloys, The Minerals, Metals & Materials Society, pp. 235-244, 2012.
24. ASM Handbook, Vol. 1, Properties and selection: Irons, Steels, and High Performance Alloys, Vo1. 1 10th Edition, pp. 1551-1569, 2005.
25. Kolagar, A. M., Cheraghzadeh, M., Tabrizi, N., and Shahriari, M. S., “The Effect of Service Expose on Microstructure and Creep Mechanism of Gas Turbine Blades Made of IN738LC”, Journal of Iranian Metallurgical and Materials Engineering Society, Vol. 19, No. 2, pp. 146-160, 2016.
26. Zhang, J. X., Murakumo, T., Harada, H., Koizumi, Y., and Kobayashi, T., “Creep Deformation Mechanisms in Som Modern Single-crystal Superalloys”, TMS (The Minerals, Metals and Materials Society), pp. 189-195, 2004.
27. Goehler, T., Schwalbe, C., Svoboda, J., Affeldt, E., and Singer, R. F., “Discussing the Effect of Gama Prime Coarsening on High Temperature Low Stress Creep Deformation with Respect to the Role of Refractory Elements”, TMS (The Minerals, Metals & Materials Society), pp. 655-664, 2016.
28. Cheng, K. Y., Jo, C. Y., Kim, D. H., Jin, T., and Hu, Z. Q., “Influence of Local Chemical Segregation on the γ' Directional Coarsening Behavior in Single Crystal Superalloy CMSX-4”, Materials Characterization, No. 60, pp. 210-218, 2009.
29. Epishin, A., Link, T., Brückner, U., Fedelich, B., and Portella, P. D., “Effects of Segregation in Nickel-Based Superalloys: Dendritic Stresses”, Superalloys 2004, The Minerals, Metals & Materials Society, Pennsylvania, PA, pp. 537-743, 2004.
30. Zacherl Shang, C. L., Kim, D. E., Wang, Y., and Liu, Z. K., “Effects of Alloying Elements on Elastic, Stacking Fault, and Diffusion Properties of FCC Ni from First-Principles: Implications for Tailoring the Creep Rate of Ni-Based Superalloys”, Superalloys 2012, 12th International symposium on superalloys, TMS (The Mineral, Metals and Materials Society, pp. 455-461, 2012.

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