سینتیک رشد لایه آستنیت در سطح فولاد زنگ‌نزن فریتی Fe-23Cr-2/4Mo حین عملیات نیتروژن‌دهی محلولی

نویسندگان

1 1- دانشکده مهندسی مواد، دانشگاه صنعتی سهند، تبریز

2 2- گروه مهندسی مواد، دانشکده فنی مهندسی، دانشگاه شهید مدنی آذربایجان، تبریز

چکیده

در این تحقیق سینتیک رشد لایه آستنیت در سطح فولاد زنگ‌نزن فریتی Fe-23Cr-2/4Mo حین عملیات نیتروژن‌دهی محلولی و تأثیر افزودن نیتروژن برروی ریزساختار و سختی فولاد مورد مطالعه قرار گرفته است. تسمه‌هایی به ضخامت 2 میلی‌متر از این فولاد در دمای 1200 درجه سانتی‌گراد تحت اتمسفر گاز نیتروژن با فشار25/0 مگاپاسکال به مدت زمان‌های 2، 3، 6، 9 و 12 ساعت نیتروژن‌دهی شدند. ریزساختار، ضخامت لایه آستنیتی و سختی نمونه‌های نیتروژن‌دهی شده با استفاده از میکروسکوپ نوری، تفرق پرتو ایکس (XRD) و ریزسختی سنجی مطالعه شدند. نتایج نشان داد که با انجام عملیات نیتروژن‌دهی، نیتروژن به‌صورت مرزدانه‌ای و شبکه‌ای نفوذ کرده و باعث استحاله فازی فریت به آستنیت می‌شود. سینتیک استحاله فریت به آستنیت با نفوذ نیتروژن با ضریب نفوذ متوسط 5-10×54/6 میلی‌متر مربع بر ثانیه کنترل می‌شود. ضخامت لایه آستنیتی تشکیل شده متناسب با ریشه دوم زمان نیتروژن‌دهی افزایش می‌یابد و پس از 12 ساعت نیتروژن‌دهی، کل ضخامت نمونه فریتی با سختیHV0/1  262 به آستنیت با سختی HV0/1  420 تبدیل می‌شود.
 

کلیدواژه‌ها

عنوان مقاله [English]

Kinetics of Austenite Layer Growth on the Surface of Fe-23Cr-2.4Mo Ferritic Stainless Steel During Solution Nitriding

نویسندگان [English]

  • Kh. Farjam Hajiagha 1
  • A. R. Akbari 1
  • R. Mohammadzadeh 2
1 1. Department of Materials Engineering, Sahand University of Technology, Tabriz, Iran
2 2. Department of Engineering, Azarbayjan Shahid Madani University, Tabriz, Iran
چکیده [English]

In this study, the kinetics of austenite layer growth on the surface of Fe-23Cr-2.4Mo ferritic stainless steel during solution nitriding and the effects of nitrogen adding on microstructure and hardness of the steel have been investigated. Steel plates of 2 mm thick were solution-nitrided at 1200˚C under nitrogen pressure of 0.25 MPa for 2, 3, 6, 9, 12 hours. Microstructure, the thickness of austenite layer and the hardnes of the nitrided samples, were investigated by using optical microscope, X-ray Diffraction (XRD) and microhardness measurements. The results showed that during solution nitriding, nitrogen diffuses through the lattice and grain boundaries and transforms ferrite to austenite phase, with average nitrogen diffusion coefficient of 6.54×10-5 mm2s-1. The thickness of the austenite layer formed on the samples surfaces increased proportional to the square root of the nitriding time, so that after 12 hours niriding, the whole thickness of the ferritic sample with hardness of 262 HV0.1 transformed to austenite with hardness of 420 HV0.1.

کلیدواژه‌ها [English]

  • Solution Nitriding
  • phase transformation
  • Austenite Layer Thickness
  • Ferritic Stainless Steel
  • Microhardness

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مواد پیشرفته در مهندسی
دوره 36، شماره 2
شهریور 1396
صفحه 55-66

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