بررسی تشکیل نانوذرات آلومینا در زمینه مس به‌روش آلیاژسازی مکانیکی مس-1% آلومینیوم و اکسید مس

نویسندگان

گروه مهندسی مواد، دانشگاه شهید باهنر کرمان

چکیده

استحکام بخشی مس با توزیع اکسید در آن به‌عنوان یک روش کارآمد برای افزایش استحکام مس بدون کاهش جدی در هدایت الکتریکی و گرمایی آن، شناخته شده است. چنین کامپوزیتی می تواند دماهای خیلی بالا را تحمل کند و خواص خود را حفظ کند. اینگونه آلیاژها کاربردهای زیادی علی‌الخصوص در دماهای بالا شامل الکترودهای جوشکاری مقاومتی، موتورهای الکتریکی و سویچ ها دارند. در تحقیق حاضر، ابتدا محلول جامد مس- 1% آلومینیوم با آلیاژسازی مکانیکی تحت 48 ساعت آسیاکاری، آماده شد. سپس 66/0 گرم پودر اکسید مس به محلول جامد مس- 1% آلومینیوم اضافه شد و در زمان‌های 0، 16، 32 و48 ساعت مورد آسیاکاری قرار گرفت. مخلوط پودری آسیا شده با تکنیک‌های پراش پرتو ایکس و میکروسکوپ الکترونی روبشی مورد بررسی قرار گرفت؛ پارامتر شبکه مس با افزایش زمان آسیا‌کاری ابتدا افزایش و سپس کاهش می‌یابد. روند تغییرات کرنش کاملاً افزایشی و روند تغییرات اندازه کریستال کاملاً کاهشی بود. اندازه ذرات روند کاملاً کاهشی نشان داد. میکروسختی نمونه‌ها با افزایش دمای عملیات حرارتی از 450 درجه سانتی‌گراد به 750 درجه سانتی‌گراد روند کاهشی- افزایشی نشان داد. مجموعه این نتایج دلیلی بر تشکیل نانو‌ذرات آلومینا در زمینه مس است.
 

کلیدواژه‌ها

عنوان مقاله [English]

Evaluation of Synthesizing Al2O3 Nano Particles in Copper Matrix by Mechanical Alloying of Cu-1% Al and Copper Oxide

نویسندگان [English]

  • S. Safi
  • G. H. Akbari
  • G. H. Akbari
Department of Materials Science and Engineerig, Shahid Bahonar, Kerman, Iran
چکیده [English]

Strengthening of copper matrix by dispersion of metallic oxides particles as an efficient way to increase strength without losing thermal and electrical conductivities has been recognized for many years. Such a composite can withstand high temperatures and keep its properties. Such copper alloys have many applications especially in high temperature including resistance welding electrodes, electrical motors and switches. In the present work, at first, the Cu-1%Al solid solution was prepared by the mechanical alloying process via 48 hours of milling. Subsequently, 0.66 gr of copper oxide was added to Cu-1%Al solid solution and mechanically milled for different milling times of 0,16, 32, 48 hours. The milled powder mixtures were investigated by X-Ray Diffraction and scanning electron microscopy techniques. The lattice parameter of Cu increased at first, but then decreased at longer milling times. The internal strain increased and the average Cu crystal size decreased during milling process.The particle size decreased during the whole process. With increasing annealing temprature from 450°C to 750°C, the microhardness values of samples decreased at the beginning but then increased. From these results, it can be concluded that nanosize aluminaparticles are formed in the copper matrix.

کلیدواژه‌ها [English]

  • Solid Solution
  • Cu-Al
  • mechanical alloying
  • X-Ray diffraction
  • Scanning Electron Microscopy (SEM)
  • Microhardness
  • Alumina

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مواد پیشرفته در مهندسی
دوره 36، شماره 1
خرداد 1396
صفحه 71-85

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