سنتز و مشخصه‌یابی ساختاری، مغناطیسی و الکترومغناطیسی کامپوزیت‌های فریت کبالت / اکسیدگرافن احیاشده

نویسندگان

گروه فیزیک دانشکده علوم پایه، دانشگاه ملایر، ایران

چکیده

در این پژوهش پودر فریت کبالت (CoFe2O4) و نیز کامپوزیت فریت کبالت / اکسیدگرافن احیاشده (CoFe2O4/RGO) با پیش‌ماده‌های کلریدی به روش هم-رسوبی سنتز شد و ساختار فازی، ریخت، ویژگی‌های مغناطیسی و جذب امواج ماکروویو آن در نوار ایکس بررسی شد. آزمون پراش پرتو ایکس نشان‌دهنده‌ تشکیل تک فاز CoFe2O4 و همه قله‌های اصلی به فاز اسپینل مربوط می‌شود. طبق تصاویر میکروسکوپی الکترونی روبشی گسیل میدانی، مورفولوژی بیشتر ذرات در CoFe2O4 و کامپوزیت CoFe2O4/RGO تقریباً کروی است. نتایج آزمون مغناطش‌سنج نمونه ارتعاشی نشان می‏دهد که مغناطش اشباع CoFe2O4 و کامپوزیت‌های دارای 5 و 10 درصد اکسیدگرافن احیاشده برابر با emu/g71/6،56 و 37 است. در آخر نتایج حاصل از تحلیل‌گر شبکه‌برداری نشان داد که بیشینه تلفات در نوار ایکس فریت کبالت برابر با dB-3/5 بوده که با افزودن 10 درصد اکسیدگرافن احیاشده به مقدار dB-21/5 رسید. همچنین میزان جذب موج تابیده شده نیز از 41 درصد برای نمونه‌ فریتی به 99/5 درصد برای نمونه‌ با 10 درصد اکسیدگرافن احیاشده رسید. 

کلیدواژه‌ها

عنوان مقاله [English]

SYNTHESIS AND STRUCTURAL, MAGNETIC, AND ELECTROMAGNETIC CHARACTERIZATION OF COBALT FERRITE / REDUCED GRAPHENE OXIDE COMPOSITE

نویسندگان [English]

  • N. Ghobadi
  • S. A. Hosseini Moradi
  • M. Amirzade
Department of Physics, Malayer University, Malayer, Iran
چکیده [English]

In this research, cobalt ferrite powders (CoFe2O4) and cobalt ferrite/reduced graphene oxide composite (CoFe2O4/RGO) were synthesized by the co-precipitation method. The phase structure, morphology, magnetic properties, and microwave absorption properties of the produced samples were investigated through various techniques. X-ray diffraction test indicated the successful formation of pure CoFe2O4  and its composites with RGO. According to the Scanning electron microscopy (SEM) images, most pure and composite samples’ particles were formed in a semi-spherical shape. The VNA test results showed the saturation magnetization of CoFe2O4 and the composite containing 5 wt.% and 10 wt.% of RGO, 71.6, 56, and 37 emu/g, respectively. Also, the network analyzer results demonstrated the maximum reflective losses in the X-band range due to the impact of microwaves on CoFe2O4 te was -5.5 db. This amount reached 21.5 dB with the addition of 10 wt.% RGO. Also, the wave input increased from 41% for the pure CoFe2O4 to 99.5% for the sample containing 10 wt.% RGO.

کلیدواژه‌ها [English]

  • Cobalt Ferrite
  • Reduced graphene oxide
  • composite
  • Reflective losses

مراجع

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مواد پیشرفته در مهندسی
دوره 40، شماره 4
اسفند 1400
صفحه 69-83

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