بررسی اثر محیط بر سنتز نانوذرات نیکل و اکسید نیکل به روش فرسایش لیزری با لیزر فیبری نانوثانیه

نوع مقاله : مقاله پژوهشی

نویسندگان

1 دانشگاه صنعتی مالک اشتر، مجتمع دانشگاهی مواد و فناوری‌های ساخت، ایران

2 دانشکده مهندسی مواد، دانشگاه صنعتی امیرکبیر، ایران

چکیده

مقدمه و اهداف: نانوذرات نیکل به دلیل خواص فیزیکی، شیمیایی و مغناطیسی، قیمت ارزان و دمای تف‌جوشی مطلوب، در چاپ الکترونیک، ساخت خازن‌های سرامیکی چندلایه، دستگاه‌های مغناطیسی و الکترودهای ابر خازن‌ها در صنعت الکترونیک استفاده می‌شود. هدف از این پژوهش سنتز نانوذرات نیکل به روش فرسایش لیزری در مایع می باشد.
مواد و روش‌ها: به‌منظور ارزیابی‌ نانوذرات سنتزشده، از میکروسکوپ الکترونی روبشی گسیل میدانی، پراش نور دینامیکی، الگوهای پراش اشعه ایکس و طیف‌سنجی نوری مرئی- فرابنفش استفاده شد.
یافته‌ها: نتایج نشان داد که نانوذرات سنتزشده در حلال آب مقطر، شامل نانوذرات نیکل با ساختار کریستالی FCC و ساختار هسته-پوسته نیکل/ اکسید نیکل (NiO/Ni) با میانگین اندازه ذرات nm 70، مورفولوژی کروی و سطح زبر است؛ اما برای نانوذرات سنتزشده در حلال حاوی پایدارکننده پلی وینیل پیرولیدون، شامل نانوذرات نیکل خالص با اندازه‌ای در حدود nm 60، مورفولوژی کروی با ساختار کریستالی FCC است. نانوذرات نیکل سنتزشده در حلال حاوی پایدارکننده پلی وینیل پیرولیدون به علت مورفولوژی مناسب، توزیع مناسب اندازه ذرات و عدم تشکیل اکسید در آن می‌تواند گزینه مناسبی برای سنتز نانوذرات نیکل باشد. 
نتیجه‌گیری: نانوذرات سنتزشده در حلال حاوی پایدارکننده پلی وینیل پیرولیدون به علت مورفولوژی مناسب، توزیع مناسب اندازه ذرات و عدم تشکیل اکسید در آن می‌تواند گزینه مناسبی برای تولید جوهرهای رسانا باشد.

کلیدواژه‌ها

موضوعات

عنوان مقاله [English]

Investigating the Effect of Environment on the Synthesis of Nickel and Nickel Oxide Nanoparticles Using the Laser Ablation Method with a Nanosecond Fiber Laser

نویسندگان [English]

  • Shahin Torkamani 1
  • Hamed Naderi-Samani 1
  • Reza Shoja Razavi 1
  • Mohammad Gavahian Jahromi 1
  • Ehsan Naderi-Samani 1
  • Mohammad Reza Borhnai 1
  • Atefeh Heidarian 2
1 Faculty of Materials and Manufacturing Technologies, Malek Ashtar University of Technology, Iran
2 Faculty of Materials and Metallurgical Engineering, Amirkabir University of Technology, Iran
چکیده [English]

Introduction and Objectives: Nickel nanoparticles are utilized in electronic printing, multilayer ceramic capacitors, magnetic devices, and supercapacitor electrodes in the electronics industry due to their favorable physical, chemical, and magnetic properties, low cost, and optimal sintering temperature. The objective of this study is to synthesize nickel nanoparticles via laser ablation in liquid.
Materials and Methods: To characterize the synthesized nanoparticles, field-emission scanning electron microscopy, dynamic light scattering, X-ray diffraction, and ultraviolet-visible spectroscopy were employed.
Results: The results revealed that nanoparticles synthesized in distilled water consisted of nickel nanoparticles with FCC crystalline structure and a nickel/nickel oxide (Ni/NiO) core-shell structure. These particles exhibited an average size of 70 nm, spherical morphology, and a rough surface. In contrast, nanoparticles synthesized in a solvent containing Polyvinylpyrrolidone as a stabilizer comprised pure nickel nanoparticles with an average size of 60 nm, spherical morphology, and an FCC crystalline structure. The Polyvinylpyrrolidone-stabilized nanoparticles, owing to their uniform morphology, narrow particle size distribution, and absence of oxide formation, are a promising candidate for nickel nanoparticle synthesis.
Conclusion: The nickel nanoparticles synthesized in the Polyvinylpyrrolidone-containing solvent, due to their optimal morphology, uniform particle size distribution, and lack of oxide formation, are well-suited for the production of conductive inks.

کلیدواژه‌ها [English]

  • Laser ablation
  • Nickel nanoparticle synthesis
  • Polyvinylpyrrolidone (PVP) stabilizer
  • Nanosecond laser

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